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1 March 1992 Hydrogen bonding in crystalline beta-D-fructopyranose: a deuterium exchange and variable low-temperature FTIR study
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Proceedings Volume 1575, 8th Intl Conf on Fourier Transform Spectroscopy; (1992) https://doi.org/10.1117/12.56333
Event: Eighth International Conference on Fourier Transform Spectroscopy, 1991, Lubeck-Travemunde, Germany
Abstract
Variable temperature FT-IR spectra have been recorded of (beta) -D-fructopyranose in the range from 300 to 110 K. The drastic natural resolution enhancement showing up in the OH- stretching region upon cooling yields detailed information with respect to the H-bonded system in the crystalline phase. Based on deuterium exchange experiments we have shown experimentally the presence of vibrational coupling between some of the H-bonded OH groups. Using the spectral information of the noncoupled OH stretching vibrations we have made a tentative assignment in the OH-stretching region.
© (1992) COPYRIGHT Society of Photo-Optical Instrumentation Engineers (SPIE). Downloading of the abstract is permitted for personal use only.
E. T.G. Lutz, J. S.J. Veldhuizen, Hendrik J. Luinge, John H. van der Maas, J. Baran, and H. Ratajczak "Hydrogen bonding in crystalline beta-D-fructopyranose: a deuterium exchange and variable low-temperature FTIR study", Proc. SPIE 1575, 8th Intl Conf on Fourier Transform Spectroscopy, (1 March 1992); https://doi.org/10.1117/12.56333
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