A novel technique for preparing a mono-particle layer on a substrate through the epoxy-amino cross-linking

Shogo Onishi; Kazufumi Ogawa

doi:10.1117/12.695415

20 December 2006 A novel technique for preparing a mono-particle layer on a substrate through the epoxy-amino cross-linking

Shogo Onishi, Kazufumi Ogawa

Author Affiliations +

Proceedings Volume 6415, Micro- and Nanotechnology: Materials, Processes, Packaging, and Systems III; 64150W (2006) https://doi.org/10.1117/12.695415
Event: SPIE Smart Materials, Nano- and Micro-Smart Systems, 2006, Adelaide, Australia

Abstract

We present a novel technique for immobilizing nanoparticles on a substrate. This method contains two techniques, which are a preparing technique of self-assembled monomolecular layers (SAMs) terminated in an epoxy group or an amino group on surface of nanoparticles or a substrate and a reaction technique between the epoxy and amino groups. The epoxy terminated SAMs or the amino terminated SAMs were prepared on nanoparticle surfaces or a substrate surface by a chemical adsorption technique using 3-glycidoxypropyltrimethoxysilane or (3-aminopropyl) trimethoxysilane. The particles dispersed in an organic solvent were coated on the substrate, and then the epoxy and amino groups were reacted each other. Unreacted nanoparticles were removed by washing. As a result, the nanoparticles were immobilized to the substrate surface through covalent bonds of the epoxy-amine cross-linking. By using this method, a mono nanoparticle layer could be formed on the substrate.

Citation Download Citation

Shogo Onishi and Kazufumi Ogawa "A novel technique for preparing a mono-particle layer on a substrate through the epoxy-amino cross-linking", Proc. SPIE 6415, Micro- and Nanotechnology: Materials, Processes, Packaging, and Systems III, 64150W (20 December 2006); https://doi.org/10.1117/12.695415

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