Preparation of P(DVB-co-MPS) inorganic-organic hybrid polymer microspheres

Chunrong Wu; Jimei Zhang; Zhao Dai; Xiaoyu Chen

doi:10.1117/12.869720

22 July 2010 Preparation of P(DVB-co-MPS) inorganic-organic hybrid polymer microspheres

Chunrong Wu, Jimei Zhang, Zhao Dai, Xiaoyu Chen

Proceedings Volume 7749, 2010 International Conference on Display and Photonics; 77490I (2010) https://doi.org/10.1117/12.869720
Event: 2010 International Conference on Display and Photonics, 2010, Nanjing, China

Abstract

A novel inorganic-organic hybrid polymer microspheres were facilely synthesised by distillation-precipitation polymerization in absence of any stabilizer or surfcant. The process were conducted with [3-(Methacryloyloxy) propyl] trimethoxysilan (MPS) as monomer, divinyl benzene (DVB) as cross linking agent and azobisisobutyronitrile (AIBN) as initator in acetonitrile. A series of silica nanoparticles were prepared in accordance with the volume ratio of MPS, which was varied in the range of 10% to 50%. However, there is no microspheres obtained while the ratio up to 50%. Products were charactered by transmission electron micrograph (TEM) and fourier transform infrared spectroscopy (FTIR). We may infer it from the constructional formular and FTIR graph that there were silicon hydroxyl remained in the microsphere surface.

Citation Download Citation

Chunrong Wu, Jimei Zhang, Zhao Dai, and Xiaoyu Chen "Preparation of P(DVB-co-MPS) inorganic-organic hybrid polymer microspheres", Proc. SPIE 7749, 2010 International Conference on Display and Photonics, 77490I (22 July 2010); https://doi.org/10.1117/12.869720

ACCESS THE FULL ARTICLE

INSTITUTIONAL
Select your institution to access the SPIE Digital Library.

SELECT YOUR INSTITUTION

PERSONAL
Sign in with your SPIE account to access your personal subscriptions or to use specific features such as save to my library, sign up for alerts, save searches, etc.

PERSONAL SIGN IN

No SPIE Account? Create one

PURCHASE THIS CONTENT

SUBSCRIBE TO DIGITAL LIBRARY

50 downloads per 1-year subscription

Members: $195

Non-members: $335 ADD TO CART

25 downloads per 1 - year subscription

Members: $145

Non-members: $250 ADD TO CART

PURCHASE SINGLE ARTICLE

Includes PDF, HTML & Video, when available