A testing method has been set up to evaluate the attenuation performance of an absorption coat to 8mm waves, which is based on a set of detecting system included by an 8mm wave emitter, a millimeter power meter, a point to point collimator and a reflecting plate. The power meter was aimed at the 8 mm wave emitter along the reflection optical path instead of the direction observation between incident and reflected millimeter wave. Some Al, Fe and aluminum alloy sample plates were made and painted by the dope which was complexed with chopped carbon fibers. A naked metal plate was first used to adjust the transmission path of the millimeter wave. Then the power meter was adjusted to phase locking after preheating, and the millimeter wave power was sampled as the background value. Then the other painted plates were tested under the same conditions. When the concentration of chopped carbon fibers is 0.5mg/ml and the thickness of the absorption coat is 0.5mm, the attenuation percentages of Al, Fe and aluminum alloy painted plates respectively is 54.29%, 58.31% and 41.12%. By the result, the reflection testing method may be widely used to measure the reflection capacity or attenuation performance of various surfaces to millimeter waves.