In this study, CNTs were used as modifiers of the epoxy matrix of quasi-isotropic carbon fibre reinforced laminates. The
prepared laminates were subjected to tensile loading and
tension-tension fatigue and, the changes in the longitudinal
resistance were monitored via a digital multimeter. In addition, Acoustic Emission and Acousto-Ultrasonic techniques
were used for monitoring the fatigue process of the laminates. The nano-enhanced laminates on the one hand exhibited
superior fatigue properties and on the other hand they demonstrated the full-potential of the material to be used as an
integrated sensor to monitor the fatigue life.
This study deals with new generation composite systems which apart from the primary reinforcement at the typical fiber
scale (~10 μm) are also reinforced at the nanoscale. This is performed via incorporation of nano-scale additives in typical
aerospace matrix systems, such as epoxies. Carbon Nanotubes (CNTs) are ideal candidates as their extremely high aspect
ratio and mechanical properties render them advantageous to other nanoscale materials. The result is the significant
increase in the damage tolerance of the novel composite systems even at very low CNT loadings. By monitoring the
resistance change of the CNT network, information both on the real time deformation state of the composite is obtained
as a reversible change in the bulk resistance of the material, and the damage state of the material as an irreversible
change in the bulk resistance of the material. The irreversible monotonic increase of the electrical resistance can be
related to internal damage in the hybrid composite system and may be used as an index of the remaining lifetime of a
structural component.
In aerospace structures, the increase of mechanical performance of materials such as Carbon Fiber Reinforced Polymers
(CFRPs) is always a key goal. In parallel, there is a constant demand for multi-functional solutions that provide
continuous, integrated damage monitoring in an efficient and cost affordable way. Structural Health Monitoring systems
are crucial for a variety of aerospace applications where safety, operational cost and the maintenance have increased
significantly. The Electrical Resistance Technique (ERT) as a promising damage monitoring technique uses the CFRP
materials themselves as inherent damage sensors. Currently method's medium sensitivity does not allow the
identification of early damage stages requested for a potential application. By using highly conductive carbon-nanotubes
as filler material into the epoxy matrix of CFRP is expected to increase the sensitivity of the method, allowing for wider
field of applications. In addition, it is expected that the introduction of CNTs into the polymer matrix of CFRP laminates
will increase the overall mechanical and electrical performance of the composite. This double role of the CNTs is
investigated in the present study. Quasi-static tensile, cyclic loading-unloading-reloading with increase load level at each
loading cycle and tension-tension fatigue tests with parallel monitoring of the longitudinal resistance performed on
CFRP laminates with various contents of CNTs in the epoxy matrix showed that matrix cracking and fiber breakage
caused resistance to increase irreversibly. Although the individual damage mechanisms could not be easily distinguished
the overall damage state can be reliably characterized. Moreover significant increase in the fracture resistance was
shown, for both Mode I and Mode II tests in the case of CNT doped laminates, compared against the reference laminate
where neat epoxy matrix was used. Finally, low velocity impact tests showed that the CNT doped laminates appear to
have reduced damage area based on C-Scan evidences.
Conference Committee Involvement (1)
Second International Conference on Smart Materials and Nanotechnology in Engineering
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