Paper
16 May 2007 Microstructure fibers for sensing gaseous hydrocarbons
Author Affiliations +
Abstract
The paper presents new experimental results on the sensitivity of three types of microstructure fibers (MSFs) modified by xerogel layers to aromatic hydrocarbons, namely to toluene. MSFs with air holes with diameters in a range 10 - 50 &mgr;m, arranged in one, two or three rings, were prepared and their segments were used in sensing experiments. Capillary silica fibers (CFs) were also fabricated for reference sensing measurements. Segments of the fabricated MSFs and CFs were modified by thin xerogel layers applied onto the hole walls by the sol-gel method from sols based on tetraethoxysilane or methyltriethoxysilane. For sensing experiments, the segments were fixed in a special cell making it possible to control the excitation of the fiber and flow of gaseous chemicals through the air holes. The sensitivity of the MSFs and SCFs to gaseous mixtures of toluene in nitrogen was determined from spectral changes of the output light from the fibers in a range of 1600-1800 nm. Experimental results show that the sensitivity of MSFs depends on their architecture, particularly on the arrangement, diameters and number of air holes. A detection limit of about 0.007 vol.% of toluene has been achieved.
© (2007) COPYRIGHT Society of Photo-Optical Instrumentation Engineers (SPIE). Downloading of the abstract is permitted for personal use only.
Vlastimil Matejec, Jan Mrazek, Ondrej Podrazky, Jiri Kanka, Ivan Kasik, and Marie Pospisilova "Microstructure fibers for sensing gaseous hydrocarbons", Proc. SPIE 6585, Optical Sensing Technology and Applications, 658511 (16 May 2007); https://doi.org/10.1117/12.722673
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KEYWORDS
Optical fibers

Capillaries

Californium

Sensors

Biological and chemical sensing

Calibration

Silica

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